p-methoxyphenyl phosphorodichloridite

Base Information

• Chemical Name: p-methoxyphenyl phosphorodichloridite
• CAS No.: 135263-41-1
• Molecular Formula: C₇H₇Cl₂O₂P
• Molecular Weight: 225.011

Synonyms:p-methoxyphenyl phosphorodichloridite

Chemical Property of p-methoxyphenyl phosphorodichloridite

Chemical Property:

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Technology Process of p-methoxyphenyl phosphorodichloridite

There total 1 articles about p-methoxyphenyl phosphorodichloridite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-phenol (150-76-5) → p-methoxyphenyl phosphorodichloridite (135263-41-1)

Guidance literature:

With phosphorus trichloride; zuletzt Behandeln bei 50-60grad;

Reference yield: 68.0%

p-methoxyphenyl phosphorodichloridite (135263-41-1) + (S)-2,2',3,3'-tetrahydro-1,1'-spirobi[indene]-7,7'-diol → 4-methoxyphenyl-[(S)-1,1'-spirobiindane-7,7'-diyl]-phosphite

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1021/ol060360c

Reference yield: 67.0%

2,2,2-trifluoroethanol (75-89-8) + p-methoxyphenyl phosphorodichloridite (135263-41-1) → 4-methoxyphenylbis(2,2,2-trifluoroethyl)phosphite

Guidance literature:

With triethylamine; In hexane; at -30 - 22 ℃; Inert atmosphere;

DOI:10.1134/S1070363220050138

upstream raw materials:

4-methoxy-phenol

Downstream raw materials:

tetrachloro-(4-methoxy-phenoxy)-phosphorane

C₁₇H₂₀N₅O₇P

3'-azidothymidine 5'-[p-methoxyphenyl methoxyalaninyl phosphate]

2',3'-didehydro-2',3'-dideoxythymidine 5'-(4-methoxyphenyl (methoxyalaninyl)phosphate)

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