Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

Base Information

Chemical Name:Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester
CAS No.:143288-86-2
Molecular Formula:C₂₁H₂₁NO₄
Molecular Weight:351.402
Hs Code.:

Synonyms:Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

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Chemical Property of Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

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Technology Process of Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

There total 1 articles about Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-18-6
formic acid

: 101977-77-9
<3S,4S(E)>-3-<1(S)-hydroxyethyl>-1-(4-methoxyphenyl)-4-(2-phenylethenyl)-2-azetidinone

: 143288-86-2
Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1021/jo00047a020

Reference yield: 82.0%

: 143288-86-2
Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

: 101977-78-0
<3S,4S(E)>-3-<1(R)-hydroxyethyl>-1-(4-methoxyphenyl)-4-(2-phenylethenyl)-2-azetidinone

Guidance literature:: With sodium hydroxide; In ethanol; for 2h;
DOI:10.1021/jo00047a020

Reference yield:

: 143288-86-2
Formic acid (S)-1-[(3S,4S)-1-(4-methoxy-phenyl)-2-oxo-4-((E)-styryl)-azetidin-3-yl]-ethyl ester

: 143288-95-3
<1S-(1α,2α,4β,6α)>-7-(p-methoxyphenyl)-2-methyl-4-phenyl-3-oxa-7-azabicyclo<4.2.0>octan-8-one

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / 1.0 N aq. NaOH / ethanol / 2 h

2: 47 percent / p-TsOH / CH₂Cl₂ / a) 0 deg C, 1.5 h, b) to room temperature, 15 h

3: 59 percent / n-Bu₃SnH, AIBN / 2 h / 70 °C

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; toluene-4-sulfonic acid; In ethanol; dichloromethane;
DOI:10.1021/jo00047a020