(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

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Chemical Name:(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde
CAS No.:1233705-46-8
Molecular Formula:C₂₂H₃₀N₂O₆Si
Molecular Weight:446.575
Hs Code.:

Synonyms:(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

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Chemical Property of (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

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Technology Process of (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

There total 1 articles about (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₄N₅O₉Si⁽¹⁺⁾*Cl^(1-)

: 1233705-46-8
(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

Guidance literature:: With dimethyl amine; In methanol; ethanol; N,N-dimethyl-formamide; at 50 - 65 ℃; Inert atmosphere;
DOI:10.1021/ol101035p

Reference yield: 64.0%

: 1233705-46-8
(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

: 124-40-3
dimethyl amine

: 1233705-47-9
(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

Guidance literature:: (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde; With sodium cyanide; In tetrahydrofuran; isopropyl alcohol; at 0 ℃; for 0.0833333h; Inert atmosphere;

dimethyl amine; In tetrahydrofuran; isopropyl alcohol; at 0 ℃; for 0.166667h; Inert atmosphere;

With manganese(IV) oxide; In tetrahydrofuran; isopropyl alcohol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101035p