(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

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Chemical Name:(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide
CAS No.:1233705-47-9
Molecular Formula:C₂₄H₃₅N₃O₆Si
Molecular Weight:489.644
Hs Code.:

Synonyms:(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

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Chemical Property of (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

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Technology Process of (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

There total 1 articles about (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1233705-46-8
(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde

: 124-40-3
dimethyl amine

: 1233705-47-9
(E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]-N,N-dimethylacrylamide

Guidance literature:: (E)-3-[(S)-5-((tert-butyldimethylsilyloxy)methyl)-1-(3-methoxy-2-nitrobenzoyl)-4,5-dihydro-1H-pyrrol-3-yl]acrylaldehyde; With sodium cyanide; In tetrahydrofuran; isopropyl alcohol; at 0 ℃; for 0.0833333h; Inert atmosphere;

dimethyl amine; In tetrahydrofuran; isopropyl alcohol; at 0 ℃; for 0.166667h; Inert atmosphere;

With manganese(IV) oxide; In tetrahydrofuran; isopropyl alcohol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101035p