chlorodimesitylstibane

Base Information

Chemical Name:chlorodimesitylstibane
CAS No.:106870-55-7
Molecular Formula:C₁₈H₂₂ClSb
Molecular Weight:395.576
Hs Code.:

Synonyms:chlorodimesitylstibane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chlorodimesitylstibane

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Technology Process of chlorodimesitylstibane

There total 3 articles about chlorodimesitylstibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 23822-17-5
tris(2,4,6-trimethylphenyl)antimony

: 10025-91-9
antimony(III) chloride

: 106870-56-8
mesitylantimony dichloride

: 106870-55-7
chlorodimesitylstibane

Guidance literature:: In neat (no solvent); stirring ((CH3)3C6H2)3Sb (12 mmol) and SbCl3 (6 mmol) at 80-100°C for 12 h (Ar-atmosphere); taking up react. mixt. in n-pentane/CCl4 50:50 vol.% (2 times); cooling combined solns. to -15°C;; pptn. of ((CH3)3C6H2)SbCl2; decanting, removing solvent; taking up residual liquid in n-pentane, cooling to -15°C, pptn. of ((CH3)3C6H2)2SbCl; elem. anal.;;