4-nitrobenzene

Base Information

• Chemical Name: 4-nitrobenzene
• CAS No.: 73178-10-6
• Molecular Formula: C₁₃H₁₂INO₆S
• Molecular Weight: 437.212

Synonyms:4-nitrobenzene

Chemical Property of 4-nitrobenzene

Chemical Property:

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Technology Process of 4-nitrobenzene

There total 3 articles about 4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-nitrobenzene (64846-47-5) + toluene-4-sulfonic acid (104-15-4) → 4-nitrobenzene (73178-10-6)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1002/mrc.1260270902

Reference yield: 86.0%

p-nitrobenzene iodide (636-98-6) + toluene-4-sulfonic acid (104-15-4) → 4-nitrobenzene (73178-10-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 60 ℃; for 2h;

DOI:10.1002/chem.201502995

Reference yield:

p-nitrobenzene iodide (636-98-6) + [hydroxy(tosyloxy)iodo]benzene (27126-76-7) → 4-nitrobenzene (73178-10-6)

Guidance literature:

DOI:10.1021/jo01296a049

upstream raw materials:

p-nitrobenzene iodide

[hydroxy(tosyloxy)iodo]benzene

4-nitrobenzene

toluene-4-sulfonic acid

Downstream raw materials:

p-nitrophenylbenzoate

(4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate

1,2,5-tri-(4-nitrophenyl)-1H-pyrazole

(4-nitrophenyl)(2,4,6-trimethylphenyl)iodonium tosylate

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