4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID

Base Information

• Chemical Name: 4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID
• CAS No.: 82366-55-0
• Molecular Formula: C9H8N3O6-
• Molecular Weight: 255.187
• Hs Code.: 2922499990
• Mol file: 82366-55-0.mol

Synonyms:4-Dimethylamino-3,5-dinitro-benzoesaeure;4-dimethylamino-3,5-dinitro-benzoic acid;N,N-dimethyl-4-carboxy-2,6-dinitroaniline;

Chemical Property of 4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID

Chemical Property:

• Vapor Pressure: 5.71E-08mmHg at 25°C
• Melting Point: 248-250oC
• Boiling Point: 424.7°Cat760mmHg
• Flash Point: 210.6°C
• PSA: 132.18000
• Density: 1.559g/cm³
• LogP: 2.31360

Purity/Quality:

99% ^*data from raw suppliers

4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: R36/37/38:Irritating to eyes, respiratory system and skin.
• Statements: R36/37/38:Irritating to eyes, respiratory system and skin.
• Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36:Wear suitable prot

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 4-Dimethylamino-3,5-dinitrobenzoic Acid is used in the microbiological production of ramulosin, a germination inhibitor. Separation and identification of normal aliphatic alcohols.

Technology Process of 4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID

There total 2 articles about 4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl amine (124-40-3) + 4-chloro-3,5-dinitrobenzoic acid (118-97-8) → N,N-dimethyl-4-carboxy-2,6-dinitroaniline (82366-55-0)

Guidance literature:

With ethanol;

Reference yield:

para-chlorobenzoic acid (74-11-3) → N,N-dimethyl-4-carboxy-2,6-dinitroaniline (82366-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated sulfuric acid; nitric / 70 - 100 °C / dann bis 140grad erhitzen

2: alcohol

With ethanol; sulfuric acid; nitric acid;

Reference yield: 74.0%

N,N-dimethyl-4-carboxy-2,6-dinitroaniline (82366-55-0) + 4-chloro-aniline (106-47-8) → N-(4-chlorophenyl)-4-(dimethylamino)-3,5-dinitrobenzamide

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2019.03.035

upstream raw materials:

dimethyl amine

4-chloro-3,5-dinitrobenzoic acid

para-chlorobenzoic acid

Downstream raw materials:

4-dimethylamino-3,5-dinitro-benzoyl chloride

4-dimethylamino-3,5-dinitro-benzoyl azide