methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

Base Information

Chemical Name:methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate
CAS No.:17015-46-2
Molecular Formula:C₁₆H₂₆O₃
Molecular Weight:266.381
Hs Code.:

Synonyms:methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

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Technology Process of methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

There total 56 articles about methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86272-38-0
(S)-4-[(S)-2-(2-Isobutyl-[1,3]dithian-2-yl)-1-methyl-ethyl]-cyclohex-1-enecarboxylic acid methyl ester

: 17015-46-2
methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

Guidance literature:: With silver nitrate; In methanol;
DOI:10.1021/ja00354a049

Reference yield:

: 67-56-1
methanol

: 26462-78-2,26666-85-3,42719-55-1,51619-87-5,51619-88-6
(R)-4-(1,5-Dimethyl-3-oxo-hexyl)-cyclohex-1-enecarbaldehyde

: 16981-74-1,17015-46-2,17904-27-7,19908-46-4,26462-72-6,26462-74-8,26575-87-1,82079-49-0,82079-50-3,120019-21-8
Juvabion

Guidance literature:: With manganese(IV) oxide; sodium cyanide; acetic acid; Ambient temperature;
DOI:10.1016/S0040-4039(00)91276-0

Reference yield:

: 68075-96-7
lithio-2-(2-methylpropyl)-1,3-dithiane

: 17015-46-2
methyl (+/-)-rel-(4R)-4-[(1R)-1,5-dimethyl-3-oxoethyl]cyclohex-1-enecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / 0.75 h / -78 - 0 °C

2: 10percent aq. HCl / tetrahydrofuran / 24 h / Ambient temperature

3: NaH

4: NaBH₄ / ethanol

5: Et₃N / CH₂Cl₂

6: NaOCH₃ / benzene

7: 90 percent / AgNO₃ / methanol

With hydrogenchloride; sodium tetrahydroborate; sodium methylate; sodium hydride; silver nitrate; triethylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;
DOI:10.1021/ja00354a049