C₃₂H₄₅N₃O₁₁SSi

Base Information Edit

Chemical Name:C₃₂H₄₅N₃O₁₁SSi
CAS No.:1201905-45-4
Molecular Formula:C₃₂H₄₅N₃O₁₁SSi
Molecular Weight:707.874
Hs Code.:
Mol file:1201905-45-4.mol

C<sub>32</sub>H<sub>45</sub>N<sub>3</sub>O<sub>11</sub>SSi

Synonyms:C₃₂H₄₅N₃O₁₁SSi

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Chemical Property of C₃₂H₄₅N₃O₁₁SSi Edit

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Technology Process of C₃₂H₄₅N₃O₁₁SSi

There total 20 articles about C₃₂H₄₅N₃O₁₁SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1257051-37-8
N-[2-((5R,6R)-5-(tert-butyldimethylsilyloxy)-6-(3-(2,2-dimethoxyethyl)-2-iodo-6-methoxyphenoxy)cyclohex-1-enyl)]-N-methyl-2,4-dinitrobenzenesulfonamide

: 1201905-45-4
C₃₂H₄₅N₃O₁₁SSi

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; In acetonitrile; at 85 ℃; for 2h;
DOI:10.1002/asia.201000458

Reference yield:

: 1201905-44-3
benzyl N-[2-[(5aR,6R,9aS)-6-(tert-butyldimethylsilyloxy)-6,7-dihydro-1-(2,2-dimethoxyethyl)-4-methoxy-9a(5aH)-dibenzofuranyl]ethyl]carbamate

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 1201905-45-4
C₃₂H₄₅N₃O₁₁SSi

Guidance literature:: benzyl N-[2-[(5aR,6R,9aS)-6-(tert-butyldimethylsilyloxy)-6,7-dihydro-1-(2,2-dimethoxyethyl)-4-methoxy-9a(5aH)-dibenzofuranyl]ethyl]carbamate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 70 ℃; for 1h;

2,4-dinitrobenzenesulfonyl chloride; With sodium hydroxide; In tetrahydrofuran; diethyl ether; water; at 20 ℃; for 0.166667h;
DOI:10.1002/asia.201000458

Reference yield:

: 916225-97-3
2-iodo-6-methoxy-3-(2,2-dimethoxyethyl)phenol

: 1201905-45-4
C₃₂H₄₅N₃O₁₁SSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 0.5 h / 20 °C

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; tris-(o-tolyl)phosphine / acetonitrile / 1 h / 85 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 70 °C

3.2: 0.17 h / 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; tributylphosphine; triethylamine; tris-(o-tolyl)phosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; acetonitrile; 1.1: Mitsunobu reaction / 2.1: Heck reaction;
DOI:10.1002/asia.201000458