bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

Base Information

Chemical Name:bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate
CAS No.:697802-86-1
Molecular Formula:C₃₄H₅₁NO₉Si
Molecular Weight:645.866
Hs Code.:

bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

Synonyms:bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

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Chemical Property of bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

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Technology Process of bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

There total 1 articles about bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 581100-24-5
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

: 697802-86-1
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

Guidance literature:: bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride; With (S)-[(2R)-5-ethenyl-1-azabicyclo[2.2.2]oct-2-yl](6-methoxyquinolin-4-yl)methanol; In tetrachloromethane; toluene; at -65 ℃; for 1h;

methanol; In tetrachloromethane; toluene; at -65 ℃; for 96.5h;

Reference yield:

: 697802-86-1
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 581100-25-6
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-(trimethylsilylethoxycarbonyl)amino-5-exo-methyl dicarboxylate

Guidance literature:: bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate; With diphenyl phosphoryl azide; triethylamine; In benzene; for 24h; Heating / reflux;

2-(Trimethylsilyl)ethanol; In benzene; for 48h; Heating / reflux;