bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

Base Information

Chemical Name:bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride
CAS No.:581100-24-5
Molecular Formula:C₃₃H₄₇NO₈Si
Molecular Weight:613.824
Hs Code.:

bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

Synonyms:bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

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Chemical Property of bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

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Technology Process of bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

There total 1 articles about bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 581100-23-4
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-5-exo-methyl-6-exo-methyl tricarboxylate

: 581100-24-5
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

Guidance literature:: bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-5-exo-methyl-6-exo-methyl tricarboxylate; With formic acid; toluene-4-sulfonic acid; at 90 ℃;

With acetic anhydride; In formic acid; for 6h; Heating / reflux;

Reference yield:

: 67-56-1
methanol

: 581100-24-5
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride

: 697802-86-1
bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthyl-6-exo-carboxy-5-exo-methyl dicarboxylate

Guidance literature:: bicyclo[2.2.1]heptane-7-syn-(benzyloxy)-2-exo-(trimethylsilylethoxycarbonyl)-amino-3-endo-(L)-menthylcarbox-5-exo-6-exo-dicarboxylic anhydride; With (S)-[(2R)-5-ethenyl-1-azabicyclo[2.2.2]oct-2-yl](6-methoxyquinolin-4-yl)methanol; In tetrachloromethane; toluene; at -65 ℃; for 1h;

methanol; In tetrachloromethane; toluene; at -65 ℃; for 96.5h;