10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

Base Information

• Chemical Name: 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine
• CAS No.: 168172-74-5
• Molecular Formula: C₁₉H₁₃BrClNO₃S
• Molecular Weight: 450.74

Synonyms:10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

Chemical Property of 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

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Technology Process of 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

There total 1 articles about 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dmap (1122-58-3) + 8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine (2244-59-9) + 4-bromobenzenesulfonyl chloride (98-58-8) → 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine (168172-74-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In hexane; chloroform; ethyl acetate;

Reference yield:

4-(aminomethyl)pyridine (3731-53-1) + bis(triphenylphosphine)palladium(II) dichloride + 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine (168172-74-5) → 4-[(8-chlorodibenz[b,f][1,4]oxazepin-10(11H)-yl)sulfonyl]-N-(4-pyridinylmethyl)benzamide, monohydrochloride (168172-77-8)

Guidance literature:

With tributyl-amine; In methanol; ethyl acetate;

Reference yield:

4-pyridylacetylene (2510-22-7) + bis(triphenylphosphine)palladium(II) dichloride + 10-[(4-bromophenyl)sulfonyl]-8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine (168172-74-5) → 8-chloro-10,11-dihydro-10-[[4-[(4-pyridinyl)ethynyl]phenyl]sulfonyl]dibenz[b,f][1,4]-oxazepine (168172-75-6)

Guidance literature:

With triethylamine; In hexane; ethyl acetate;

upstream raw materials:

dmap

8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine

4-bromobenzenesulfonyl chloride

Downstream raw materials:

4-[(8-chlorodibenz[b,f][1,4]oxazepin-10(11H)-yl)sulfonyl]-N-(4-pyridinylmethyl)benzamide, monohydrochloride

8-chloro-10,11-dihydro-10-[[4-[(4-pyridinyl)ethynyl]phenyl]sulfonyl]dibenz[b,f][1,4]-oxazepine

3-[(8-chlorodibenz[b,f][1,4]oxazepin-10(11H)-yl)carbonyl]-N-(4-pyridinylmethyl)benzamide, monohydrochloride

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