2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

Base Information

Chemical Name:2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester
CAS No.:724461-52-3
Molecular Formula:C₂₃H₃₀O₃Si
Molecular Weight:382.575
Hs Code.:

2-[3-(<i>tert</i>-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

Synonyms:2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

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Chemical Property of 2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

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Technology Process of 2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

There total 3 articles about 2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 724461-48-7
methyl 5-[(tert-butyldiphenylsilyl)oxy]-2-(dimethoxyphosphoryl)pentanoate

: 724461-52-3
2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 6h; Heating;
DOI:10.1016/j.tetasy.2004.04.004

Reference yield:

: 114671-83-9
1-(t-butyldiphenylsilyloxy)-3-iodopropane

: 724461-52-3
2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / sodium hydride / dimethylsulfoxide / 2.67 h / 20 °C

2: 71 percent / potassium carbonate / tetrahydrofuran / 6 h / Heating

With sodium hydride; potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetasy.2004.04.004

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 724461-52-3
2-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-acrylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / imidazole / CH₂Cl₂ / 20 °C

2: 71 percent / sodium hydride / dimethylsulfoxide / 2.67 h / 20 °C

3: 71 percent / potassium carbonate / tetrahydrofuran / 6 h / Heating

With 1H-imidazole; sodium hydride; potassium carbonate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 3: Horner-Wadsworth-Emmons reaction;
DOI:10.1016/j.tetasy.2004.04.004