(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

Base Information

Chemical Name:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)
CAS No.:1013399-74-0
Molecular Formula:C₄₃H₈₅BO₂Si₇
Molecular Weight:841.556
Hs Code.:

Synonyms:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

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Chemical Property of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

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Technology Process of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

There total 4 articles about (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 77-78-1
dimethyl sulfate

: 796870-05-8
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

: 1013399-74-0
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

Guidance literature:: With n-BuLi; In hexane; (Ar); soln. of BuLi in hexane was added to soln. of B compd. in hexane at 0°C (or -78°C); stirred at 0°C for 30 min (or at -78°C for 30 min); (MeO)2SO2 was added; solvent removed; chromd. (SiO2 plate, hexane/CHCl3, 2/1);
DOI:10.1021/om7008974

Reference yield: 58.0%

: 74-88-4
methyl iodide

: 796870-05-8
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))2

: 1013399-74-0
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

Guidance literature:: With n-BuLi; In hexane; (Ar); soln. of BuLi in hexane was added to soln. of B compd. in hexane at 0°C; stirred at 0°C for 30 min; MeI was added; solvent removed; chromd. (SiO2 plate, hexane/CHCl3, 2/1);
DOI:10.1021/om7008974

Reference yield:

: 2,4,6-tris[bis(trimethylsilyl)methyl]phenyl(mesityl)SiCN(2,4,6-tri-tert-butylphenyl)

: 1013399-74-0
(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(pinacolato))(Me)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: n-BuLi / hexane

With n-BuLi; In tetrahydrofuran; hexane;
DOI:10.1021/om7008974