(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Base Information

Chemical Name:(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid
CAS No.:1007096-37-8
Molecular Formula:C₂₈H₂₈N₂O₅
Molecular Weight:472.541
Hs Code.:

Synonyms:(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Suppliers and Price of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Iris Biotech GmbH
Fmoc-L-Lys(Bz)-OH
5 g
$ 3699.00

American Custom Chemicals Corporation
FMOC-LYS(BZO)-OH 95.00%
5MG
$ 498.20

Total 3 raw suppliers

Chemical Property of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Fmoc-L-Lys(Bz)-OH ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

There total 3 articles about (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1245942-37-3
(S)-methyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoate

: 1007096-37-8
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Guidance literature:: (S)-methyl 2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoate; With water; calcium chloride; sodium hydroxide; In isopropyl alcohol; at 20 ℃; for 5h;

With acetic acid; In water; isopropyl alcohol;
DOI:10.1016/j.bmc.2010.06.035

Reference yield:

: 23405-15-4
benzoic acid N-hydroxysuccinimide ester

: 139262-23-0
9-fluorenylmethoxycarbonyl-L-alanine hydrochloride

: 1007096-37-8
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 1007096-37-8
(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / dichloromethane / 24 h / 20 °C

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;