(S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate

Base Information

• Chemical Name: (S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate
• CAS No.: 1245942-83-9
• Molecular Formula: C₂₂H₃₂N₄O₆
• Molecular Weight: 448.519
• Mol file: 1245942-83-9.mol

Synonyms:(S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate

Chemical Property of (S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate

There total 1 articles about (S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

methanol (67-56-1) + C32H28NO5Pol + (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid (1007096-37-8) + N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine (35661-39-3,136132-75-7) + acetic acid (64-19-7,77671-22-8) → (S)-methyl 2-((S)-2-((S)-2-acetamidopropanamido)-6-benzamidohexanamido)propanoate (1245942-83-9)

Guidance literature:

C₃₂H₂₈NO₅Pol; With piperidine; In N,N-dimethyl-formamide; for 0.25h; solid phase reaction;

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h; solid phase reaction;

methanol; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; acetic acid; Further stages;

DOI:10.1016/j.bmc.2010.06.035

upstream raw materials:

methanol

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-6-benzamidohexanoic acid

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

acetic acid