Me₃GePhMeGeCl

Base Information

• Chemical Name: Me₃GePhMeGeCl
• CAS No.: 124908-62-9
• Molecular Formula: C₁₀H₁₇ClGe₂
• Molecular Weight: 317.878
• Mol file: 124908-62-9.mol

Synonyms:Me₃GePhMeGeCl

Chemical Property of Me₃GePhMeGeCl

Chemical Property:

Purity/Quality:

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Technology Process of Me₃GePhMeGeCl

There total 3 articles about Me₃GePhMeGeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

1,1,1,3,3,3-hexamethyl-2,2-diphenyl-trigermane (53421-59-3) → Me3GePhMeGeCl (124908-62-9) + hexamethyldigermane (993-52-2) + dichlorodiphenylgermane (1613-66-7)

Guidance literature:

With tetrachloromethane; In cyclohexane; byproducts: Me3GeCl; Irradiation (UV/VIS); (Ar); soln. of Ge-compound with CCl4; irradiated with a 110-W low-pressure Hg arc-lamp at room temp. for 1 h; GLC and GC-MS;

DOI:10.1016/0022-328X(90)80083-C

Reference yield: 9.0%

(Me3Ge)2GePhMe (56986-59-5) → Me3GePhMeGeCl (124908-62-9) + chlorotrimethylgermane (1529-47-1) + hexamethyldigermane (993-52-2)

Guidance literature:

With tetrachloromethane; In cyclohexane; byproducts: hexachloroethane; Irradiation (UV/VIS); 110-W low pressure Hg arc lamp, under Ar, room temp.; GLC, GC-MS; Kinetics;

DOI:10.1016/0022-328X(89)87334-6

Reference yield: 9.0%

(Me3Ge)2GePhMe (56986-59-5) → Me3GePhMeGeCl (124908-62-9) + hexamethyldigermane (993-52-2) + methylphenylgermanium dichloride (25179-00-4)

Guidance literature:

With tetrachloromethane; In cyclohexane; byproducts: Me3GeCl, C2Cl6; Irradiation (UV/VIS); (Ar); soln. of Ge-compound with CCl4; irradiated with a 110-W low-pressure Hg arc-lamp at room temp. for 1 h; GLC and GC-MS;

DOI:10.1016/0022-328X(90)80083-C

upstream raw materials:

1,1,1,3,3,3-hexamethyl-2,2-diphenyl-trigermane

(Me₃Ge)2GePhMe