(+)-(R)-1-phenylbut-3-en-1-yl acetate

Base Information

Chemical Name:(+)-(R)-1-phenylbut-3-en-1-yl acetate
CAS No.:181227-42-9
Molecular Formula:C₁₂H₁₄O₂
Molecular Weight:190.242
Hs Code.:

Synonyms:(+)-(R)-1-phenylbut-3-en-1-yl acetate

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Chemical Property of (+)-(R)-1-phenylbut-3-en-1-yl acetate

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Technology Process of (+)-(R)-1-phenylbut-3-en-1-yl acetate

There total 15 articles about (+)-(R)-1-phenylbut-3-en-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-22-5
Isopropenyl acetate

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 181227-42-9
(+)-(R)-1-phenylbut-3-en-1-yl acetate

Guidance literature:: With dicarbonylchlorido(pentabenzylcyclopentadienyl)ruthenium; potassium tert-butylate; sodium carbonate; In tetrahydrofuran; toluene; at 23 ℃; for 168h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; dynamic kinetic resolution; Enzymatic reaction;
DOI:10.1002/ejoc.201001703

Reference yield: 84.0%

: 108-22-5
Isopropenyl acetate

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 77118-87-7,936-58-3
(S)-1-Phenyl-3-buten-1-ol

: 181227-42-9
(+)-(R)-1-phenylbut-3-en-1-yl acetate

Guidance literature:: With Candida antarctica lipase B; dicarbonyl(chloro)(η⁵-pentaphenylcyclopentadienyl)ruthenium(II); potassium tert-butylate; sodium carbonate; In tetrahydrofuran; toluene; at 70 ℃; for 12h; Temperature; Time; Reagent/catalyst; enantioselective reaction; Schlenk technique; Inert atmosphere; Resolution of racemate; Enzymatic reaction;
DOI:10.1002/chem.201301980

Reference yield: 45.0%

: 108-05-4,9003-20-7
vinyl acetate

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 77118-87-7,936-58-3
(S)-1-Phenyl-3-buten-1-ol

: 181227-42-9
(+)-(R)-1-phenylbut-3-en-1-yl acetate

Guidance literature:: With Amano Pseudomonas fluorescens lipase; at 50 ℃; for 6h; Reagent/catalyst; enantioselective reaction; Catalytic behavior; Resolution of racemate; Enzymatic reaction;
DOI:10.3762/bjoc.15.42