(S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal

Base Information

• Chemical Name: (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal
• CAS No.: 353291-61-9
• Molecular Formula: C₂₂H₃₆O₅
• Molecular Weight: 380.525

Synonyms:(S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal

Chemical Property of (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal

Chemical Property:

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Technology Process of (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal

There total 2 articles about (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol (353291-60-8) → (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal (353291-61-9)

Guidance literature:

With sodium periodate; In tetrahydrofuran; water; for 1h;

DOI:10.1021/ja0106164

Reference yield:

2-((S)-1-Allyl-pentyl)-1,3-dimethoxy-5-((R)-4-methoxymethoxy-2-methyl-butyl)-benzene (246144-79-6) → (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal (353291-61-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NMO; H₂O / OsO₄ / tetrahydrofuran; acetone / 2.25 h

2: 93 percent / NaIO₄ / tetrahydrofuran; H₂O / 1 h

With sodium periodate; N-methyl-2-indolinone; water; osmium(VIII) oxide; In tetrahydrofuran; water; acetone;

DOI:10.1021/ja0106164

Reference yield: 97.0%

toluene-4-sulfonic acid hydrazide (1576-35-8) + (S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal (353291-61-9) → C29H44N2O6S

Guidance literature:

In tetrahydrofuran; for 0.333333h;

DOI:10.1021/ja0106164

upstream raw materials:

(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

2-((S)-1-Allyl-pentyl)-1,3-dimethoxy-5-((R)-4-methoxymethoxy-2-methyl-butyl)-benzene

Downstream raw materials:

(R)-4-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-3-methyl-butan-1-ol

(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butyraldehyde

C₄₂H₆₆O₄

(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

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