(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

Base Information

Chemical Name:(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol
CAS No.:246144-96-7
Molecular Formula:C₄₁H₆₆O₅
Molecular Weight:638.972
Hs Code.:

Synonyms:(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

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Chemical Property of (R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

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Technology Process of (R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

There total 10 articles about (R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 246144-95-6
C₄₃H₇₀O₆

: 246144-96-7
(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; at 60 ℃; for 0.5h; Heating;
DOI:10.1021/ja0106164

Reference yield:

: 246144-79-6
2-((S)-1-Allyl-pentyl)-1,3-dimethoxy-5-((R)-4-methoxymethoxy-2-methyl-butyl)-benzene

: 246144-96-7
(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1.1: NMO; H₂O / OsO₄ / tetrahydrofuran; acetone / 2.25 h

2.1: 93 percent / NaIO₄ / tetrahydrofuran; H₂O / 1 h

3.1: 97 percent / tetrahydrofuran / 0.33 h

4.1: Et₃N / tetrahydrofuran / 0.33 h / -78 °C

5.1: t-BuLi / diethyl ether; petroleum ether / 0.33 h / -78 °C

5.2: 73 percent / diethyl ether; petroleum ether; tetrahydrofuran / 0.5 h / -78 °C

6.1: 100 percent / aq. HCl / methanol; tetrahydrofuran / 0.5 h / 60 °C / Heating

With hydrogenchloride; sodium periodate; N-methyl-2-indolinone; water; tert.-butyl lithium; triethylamine; osmium(VIII) oxide; In tetrahydrofuran; methanol; diethyl ether; water; acetone; Petroleum ether;
DOI:10.1021/ja0106164

Reference yield:

: 353291-60-8
(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

: 246144-96-7
(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: 93 percent / NaIO₄ / tetrahydrofuran; H₂O / 1 h

2.1: 97 percent / tetrahydrofuran / 0.33 h

3.1: Et₃N / tetrahydrofuran / 0.33 h / -78 °C

4.1: t-BuLi / diethyl ether; petroleum ether / 0.33 h / -78 °C

4.2: 73 percent / diethyl ether; petroleum ether; tetrahydrofuran / 0.5 h / -78 °C

5.1: 100 percent / aq. HCl / methanol; tetrahydrofuran / 0.5 h / 60 °C / Heating

With hydrogenchloride; sodium periodate; tert.-butyl lithium; triethylamine; In tetrahydrofuran; methanol; diethyl ether; water; Petroleum ether;
DOI:10.1021/ja0106164