(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

Base Information

Chemical Name:(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol
CAS No.:353291-60-8
Molecular Formula:C₂₃H₄₀O₆
Molecular Weight:412.567
Hs Code.:

Synonyms:(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

Chemical Property:

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Technology Process of (S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

There total 1 articles about (S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 246144-79-6
2-((S)-1-Allyl-pentyl)-1,3-dimethoxy-5-((R)-4-methoxymethoxy-2-methyl-butyl)-benzene

: 353291-60-8
(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

Guidance literature:: With osmium(VIII) oxide; N-methyl-2-indolinone;
DOI:10.1021/ja991538b

Reference yield: 93.0%

: 353291-60-8
(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

: 353291-61-9
(S)-3-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-heptanal

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; for 1h;
DOI:10.1021/ja0106164

Reference yield:

: 353291-60-8
(S)-4-[2,6-Dimethoxy-4-((R)-4-methoxymethoxy-2-methyl-butyl)-phenyl]-octane-1,2-diol

: 353291-62-0
(R)-4-(4-{(1S,6S)-7-[4-((S)-1-Allyl-pentyl)-3,5-dimethoxy-phenyl]-1-butyl-6-methyl-heptyl}-3,5-dimethoxy-phenyl)-3-methyl-butyraldehyde

Guidance literature:: Multi-step reaction with 6 steps

1.1: 93 percent / NaIO₄ / tetrahydrofuran; H₂O / 1 h

2.1: 97 percent / tetrahydrofuran / 0.33 h

3.1: Et₃N / tetrahydrofuran / 0.33 h / -78 °C

4.1: t-BuLi / diethyl ether; petroleum ether / 0.33 h / -78 °C

4.2: 73 percent / diethyl ether; petroleum ether; tetrahydrofuran / 0.5 h / -78 °C

5.1: 100 percent / aq. HCl / methanol; tetrahydrofuran / 0.5 h / 60 °C / Heating

6.1: 96 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h

With hydrogenchloride; sodium periodate; tert.-butyl lithium; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; Petroleum ether; 6.1: Dess-Martin oxidation;
DOI:10.1021/ja0106164