methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

Base Information

Chemical Name:methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate
CAS No.:184176-05-4
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

Synonyms:methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

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Chemical Property of methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

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Technology Process of methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

There total 10 articles about methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 766-85-8
3-methoxy-1-iodobenzene

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 184176-05-4
methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; zinc; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ol200725m

Reference yield: 56.0%

: 766-85-8
3-methoxy-1-iodobenzene

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 915040-50-5
(2S,5S)-2,5-bis-tert-butoxycarbonylaminohexane-1,6-dioic acid dimethyl ester

: 184176-05-4
methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; dichloro bis((p-dimethylaminophenyl)-?-di-tert-butylphosphine)palladium(II); zinc; In water; at 65 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo102334c

Reference yield: 35.0%

: 2398-37-0
3-methoxyphenyl bromide

: 93267-04-0,170848-34-7,889670-02-4
N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester

: 184176-05-4
methyl (S)-2-((tert-butyloxycarbonyl)amino)-3-(3-methoxyphenyl)propanoate

Guidance literature:: N-(tert-butoxycarbonyl)-L-3-iodoalanine methyl ester; With iodine; zinc; In N,N-dimethyl-formamide; for 0.0833333h;

3-methoxyphenyl bromide; With tris-(o-tolyl)phosphine; palladium diacetate; In N,N-dimethyl-formamide; at 50 ℃; for 2h; Further stages.;
DOI:10.1016/j.tet.2007.11.031