2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl-

Base Information

Chemical Name:2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl-
CAS No.:101077-14-9
Molecular Formula:C₇H₁₁Br₂N
Molecular Weight:268.979
Hs Code.:

Synonyms:2-Propen-1-amine,2-bromo-N-(2-bromo-2-propenyl)-N-methyl- (9CI); Diallylamine, b,b'-dibromo-N-methyl- (3CI); NSC 53441

Suppliers and Price of 2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl-

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl-

There total 2 articles about 2-Propen-1-amine,2-bromo-N-(2-bromo-2-propen-1-yl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74-89-5
methylamine

: 513-31-5
2-bromoallyl bromide

: 28952-70-7
N-Methyl-2-brom-allylamin

: 101077-14-9
bis-(2-bromo-allyl)-methyl-amine

Guidance literature:: With benzene;

Reference yield:

: 74-89-5
methylamine

: 513-31-5
2-bromoallyl bromide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 28952-70-7
N-Methyl-2-brom-allylamin

: 101077-14-9
bis-(2-bromo-allyl)-methyl-amine

Guidance literature:

Reference yield:

: 101077-14-9
bis-(2-bromo-allyl)-methyl-amine

: C₁₅H₁₆BN

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / pentane; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II) / toluene / 16 h / 120 °C / Glovebox; Inert atmosphere

3.1: tetrahydrofuran; diethyl ether / 24 h / 20 °C

4.1: tetrahydrofuran / 4 h / 20 °C

With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); n-butyllithium; In tetrahydrofuran; diethyl ether; toluene; pentane;
DOI:10.1002/anie.201602840