N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

Base Information

Chemical Name:N-(2-Brom-5-chlorphenyl)benzimidoylchlorid
CAS No.:37109-01-6
Molecular Formula:C₁₃H₈BrCl₂N
Molecular Weight:329.023
Hs Code.:

Synonyms:N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

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Technology Process of N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

There total 3 articles about N-(2-Brom-5-chlorphenyl)benzimidoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 838-53-9
N-(2-Brom-5-chlorphenyl)benzamid

: 37109-01-6
N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

Guidance literature:: With phosphorus pentachloride; 1) 3 h, room temperature, 2) 1 h, 100 deg C;
DOI:10.1002/jlac.198119810715

Reference yield:

: 823-57-4
2-bromo-5-chloroaniline

: 37109-01-6
N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C

2: 87 percent / PCl₅ / 1) 3 h, room temperature, 2) 1 h, 100 deg C

With phosphorus pentachloride; N,N-dimethyl-aniline;
DOI:10.1002/jlac.198119810715

Reference yield:

: 41513-04-6
2-chloro-5-bromonitrobenzene

: 37109-01-6
N-(2-Brom-5-chlorphenyl)benzimidoylchlorid

Guidance literature:: Multi-step reaction with 3 steps

1: Raney-Ni, hydrazinhydrate

2: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C

3: 87 percent / PCl₅ / 1) 3 h, room temperature, 2) 1 h, 100 deg C

With phosphorus pentachloride; nickel; hydrazine hydrate; N,N-dimethyl-aniline;
DOI:10.1002/jlac.198119810715