[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Base Information

Chemical Name:[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt
CAS No.:1263384-41-3
Molecular Formula:C₂₀H₁₆N₇O₅S*Na
Molecular Weight:489.447
Hs Code.:

Synonyms:[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Suppliers and Price of [4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

There total 9 articles about [4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 332026-86-5
3-amino-4-(1H-benzo[d]imidazol-2-yl)-1,2,5-oxadiazole

: 1263384-41-3
[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / pyridine; methanol / 20 °C / Cooling with ice

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C / 760.05 Torr

4.1: pyridine; chlorosulfonic acid / 20 °C / Cooling with ethanol-dry ice

4.2: pH 10

With pyridine; chlorosulfonic acid; hydrogen; sodium methylate; potassium carbonate; palladium 10% on activated carbon; In pyridine; methanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 798577-91-0
3-(4-{1-[2-(4-amino-phenyl)-2-oxo-ethyl]-1H-benzoimidazol-2-yl}-furazan-3-ylamino)-propionitrile

: 1263384-41-3
[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Guidance literature:: 3-(4-{1-[2-(4-amino-phenyl)-2-oxo-ethyl]-1H-benzoimidazol-2-yl}-furazan-3-ylamino)-propionitrile; With pyridine; chlorosulfonic acid; at 20 ℃; Cooling with ethanol-dry ice;

With sodium hydroxide; In water; pH=10;

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 1263384-41-3
[4-(2-{2-[4-(2-cyano-ethylamino)furazan-3-yl]benzoimidazol-1-yl}acetyl)phenyl]sulfamic acid sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(ll) bromide / ethanol / 2 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; methanol / 3 h / 20 °C / 760.05 Torr

4.1: pyridine; chlorosulfonic acid / 20 °C / Cooling with ethanol-dry ice

4.2: pH 10

With pyridine; chlorosulfonic acid; hydrogen; potassium carbonate; copper(ll) bromide; palladium 10% on activated carbon; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide;