Technology Process of 8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
There total 8 articles about 8-azido-3,6-dioxaoctyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
barium hydroxide octahydrate; barium(II) oxide;
In
N,N-dimethyl-formamide;
for 2h;
Ambient temperature;
DOI:10.1016/0008-6215(86)80016-7
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide
2: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature
With
barium hydroxide octahydrate; toluene-4-sulfonic acid; barium(II) oxide;
In
N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / silver triflate, tetramethylurea / CH2Cl2 / 20 h / Ambient temperature
2: 76 percent / M sodium methoxide / methanol / 2 h / Ambient temperature
3: 82 percent / p-toluenesulfonic acid monohydrate / dimethylformamide
4: 95 percent / bariumoxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature
With
barium hydroxide octahydrate; sodium methylate; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; tetramethylurea; barium(II) oxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(86)80016-7
