N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

Base Information

Chemical Name:N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide
CAS No.:334970-91-1
Molecular Formula:C₂₈H₂₄IN₃O₆
Molecular Weight:625.42
Hs Code.:

Synonyms:N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

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Chemical Property of N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

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Technology Process of N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

There total 1 articles about N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 334971-59-4
N-(3,4,5-trimethoxyphenyl)-3-(5-methyl-3-(2-fluoro-5-iodo-phenyl)isoxazol-4-oyl)aminophenyl acetamide

: 334970-91-1
N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

Guidance literature:: With potassium carbonate; In DMF (N,N-dimethyl-formamide); for 17h;

Reference yield: 56.0%

: 6165-68-0
thiophene boronic acid

: 334970-91-1
N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

: N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-(thien-2-yl)-quinolin-2-on-1-yl]phenylacetamide

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; water; for 24h; Heating / reflux; Nitrogen gasification;

Reference yield: 46.0%

: 67-56-1
methanol

: 334970-91-1
N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-iodoquinolin-2-on-1-yl]phenylacetamide

: 201230-82-2
carbon monoxide

: N-3,4,5-trimethoxyphenyl-3-[3-methyl-isoxazolo[4,5-c]-1,2-dihydro-5-(methoxycarbonyl)-quinolin-2-on-1-yl]phenylacetamide

Guidance literature:: With triethylamine; palladium diacetate; In methanol; acetonitrile; at 60 ℃; for 24h; under 3102.97 Torr; Heating / reflux;