5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

Base Information

Chemical Name:5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole
CAS No.:125338-94-5
Molecular Formula:C₂₉H₄₁F₃N₄O₇SSi₂
Molecular Weight:702.899
Hs Code.:

Synonyms:5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

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Chemical Property of 5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

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Technology Process of 5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

There total 5 articles about 5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 421-83-0
trifluoromethane sulfonyl chloride

: 125338-92-3
5-benzylideneamino-4-cyano-1-<3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

: 125338-94-5
5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

Guidance literature:: With pyridine; dmap; In triethylamine; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.37.1604

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 125338-94-5
5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / dimethylformamide; various solvent(s) / 0.67 h / Ambient temperature

2: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

3: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

With pyridine; dmap; toluene-4-sulfonic acid; In triethylamine; N,N-dimethyl-formamide; benzene;
DOI:10.1248/cpb.37.1604

Reference yield:

: 100-52-7
benzaldehyde

: 125338-94-5
5-benzylideneamino-4-cyano-1-<2-O-triflyl-3,5-O-(tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl>imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: 75 percent / 4-dimethylaminopyridine, pyridine / triethylamine / 0.5 h / Ambient temperature

With pyridine; dmap; toluene-4-sulfonic acid; In triethylamine; benzene;
DOI:10.1248/cpb.37.1604