N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride

Base Information

• Chemical Name: N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride
• CAS No.: 1575626-06-0
• Molecular Formula: C₁₈H₂₇N₂O*Cl
• Molecular Weight: 322.878
• Mol file: 1575626-06-0.mol

Synonyms:N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride

Chemical Property of N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride

Chemical Property:

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Technology Process of N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride

There total 1 articles about N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2-chloroethyl methyl ether (627-42-9) + 1-(2,6-diisopropylphenyl)-1H-imidazole (25364-47-0) → N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride (1575626-06-0)

Guidance literature:

With 1,1,1,3,3,3-hexamethyl-disilazane; for 36h; Inert atmosphere; Reflux;

DOI:10.1039/c3dt52773e

Reference yield: 82.0%

(1,2-dimethoxyethane)dichloronickel(II) (29046-78-4) + N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride (1575626-06-0) → 2C18H27N2O(1+)*Cl4Ni(2-)

Guidance literature:

In tetrahydrofuran; for 16h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om5008506

Reference yield: 81.0%

nickel(II) bromide dimethoxyethane (28923-39-9) + N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride (1575626-06-0) → dibromobis[1-(2,6-diisopropylphenyl)-3-(2-methoxyethyl)-1H-imidazol-2(3H)-ylidene]nickel(II)

Guidance literature:

N-(2,6-diisopropylphenyl)-N′-ethyl methyl ether imidazolium chloride; With potassium hexamethylsilazane; In toluene; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique;

nickel(II) bromide dimethoxyethane; for 3h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om5008506

upstream raw materials:

2-chloroethyl methyl ether

1-(2,6-diisopropylphenyl)-1H-imidazole