5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Base Information

• Chemical Name: 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine
• CAS No.: 37764-95-7
• Molecular Formula: C₁₆H₁₃N₃OS
• Molecular Weight: 295.365
• Mol file: 37764-95-7.mol

Synonyms:5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property of 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

There total 4 articles about 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzoyl isothiocyanate (532-55-8) + N-methylbenzothiohydrazide (21048-05-5) → 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-95-7)

Guidance literature:

In toluene;

DOI:10.1007/BF00477454

Reference yield:

potassium thioacyanate (333-20-0) + benzoyl chloride (98-88-4) + N-methylbenzothiohydrazide (21048-05-5) → 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-95-7)

Guidance literature:

Multistep reaction; (i) MeCN, (ii) /BRN= 607301/;

Reference yield:

1-methyl-1-benzoylhydrazine (1483-24-5) + Benzoyl isothiocyanate (532-55-8) → 5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine (37764-95-7)

Guidance literature:

DOI:10.1016/S0040-4039(01)84978-9

upstream raw materials:

potassium thioacyanate

benzoyl chloride

N-methylbenzothiohydrazide

1-methyl-1-benzoylhydrazine

Downstream raw materials:

1,4-Dibenzyl-1-methylthiosemicarbazid

5-benzoylamino-3-methyl-2-phenyl-[1,3,4]thiadiazolium; chloride