5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Base Information

Chemical Name:5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine
CAS No.:136743-09-4
Molecular Formula:C₃₀H₂₄Cl₂N₂O₆S
Molecular Weight:611.502
Hs Code.:

Synonyms:5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Suppliers and Price of 5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

There total 3 articles about 5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136743-00-5
2-amino-5-benzylthiopyrazine

: 136743-09-4
5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / NaNO₂, AcOH / H₂O; dioxane / 0.17 h / 5 °C

2: 93 percent / (NH₄)2SO₄ / 1.5 h / Heating

3: 0.43 g / 0.33 h / 95 - 110 °C / 0.05 Torr

With ammonium sulfate; acetic acid; sodium nitrite; In 1,4-dioxane; water;
DOI:10.1002/jhet.5570280450

Reference yield:

: 100-53-8
phenylmethanethiol

: 136743-09-4
5-benzylthio-1-(3,5-di-O-p-chlorobenzoyl-2-deoxy-β-D-ribofuranosyl)-1,2-dihydro-2-oxopyrazine

Guidance literature:: Multi-step reaction with 4 steps

1: 10.3 g / NaOEt / dimethylformamide / 48 h / Ambient temperature

2: 46 percent / NaNO₂, AcOH / H₂O; dioxane / 0.17 h / 5 °C

3: 93 percent / (NH₄)2SO₄ / 1.5 h / Heating

4: 0.43 g / 0.33 h / 95 - 110 °C / 0.05 Torr

With ammonium sulfate; sodium ethanolate; acetic acid; sodium nitrite; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570280450