4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

Base Information

Chemical Name:4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide
CAS No.:1562381-39-8
Molecular Formula:C₁₉H₁₈N₂O₃S
Molecular Weight:354.43
Hs Code.:

Synonyms:4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

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Chemical Property of 4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

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Technology Process of 4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

There total 5 articles about 4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1562381-31-0
N-((1H-inden-2-yl)ethynyl)-N-methylmethanesulfonamide

: 586-96-9
Nitrosobenzene

: 1562381-39-8
4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

Guidance literature:: With zinc trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 60 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja412634w

Reference yield:

: 74010-34-7
2-Ethinyl-1H-inden

: 1562381-39-8
4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

Guidance literature:: Multi-step reaction with 3 steps

1: silver nitrate; 1,10-Phenanthroline / acetone / 1 h / 28 °C / Inert atmosphere

2: 1,10-Phenanthroline; potassium carbonate; copper(ll) sulfate pentahydrate / toluene / 12 h / 80 °C / Inert atmosphere; Sealed tube

3: zinc trifluoromethanesulfonate / 1,2-dichloro-ethane / 0.5 h / 60 °C / Inert atmosphere

With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; zinc trifluoromethanesulfonate; potassium carbonate; silver nitrate; In 1,2-dichloro-ethane; acetone; toluene;
DOI:10.1021/ja412634w

Reference yield:

: C₁₁H₇Br

: 1562381-39-8
4-(2-formylphenyl)-N-methyl-N-(methylsulfonyl)-N'-phenylbut-2-ynimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,10-Phenanthroline; potassium carbonate; copper(ll) sulfate pentahydrate / toluene / 12 h / 80 °C / Inert atmosphere; Sealed tube

2: zinc trifluoromethanesulfonate / 1,2-dichloro-ethane / 0.5 h / 60 °C / Inert atmosphere

With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; zinc trifluoromethanesulfonate; potassium carbonate; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja412634w