(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

Base Information

Chemical Name:(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate
CAS No.:417704-43-9
Molecular Formula:C₂₇H₂₈N₂O₅
Molecular Weight:460.53
Hs Code.:

Synonyms:(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

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Chemical Property of (3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

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Technology Process of (3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

There total 1 articles about (3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 15196-02-8
(S)-3-[(benzyloxycarbonyl)amino]-1-diazo-4-phenyl-2-butanone

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 417704-43-9
(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

Guidance literature:: With triethylamine; In acetonitrile; for 24h; Irradiation;

Reference yield:

: 417704-43-9
(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

: [(S)-3-Benzyloxycarbonylamino-1-chloro-4-phenyl-but-(Z)-ylideneamino]-acetic acid benzyl ester

Guidance literature:: With quinoline; phosphorus pentachloride; In chloroform; at 20 ℃; for 2.5h;

Reference yield:

: 417704-43-9
(3S)-benzyl 2-[4-phenyl-3-(benzyloxycarbonylamino)butanoylamino]ethanoate

: (2S)-5-(2-amino-3-phenylpropyl)-1-[(methyl L-valinyl-L-isoleucinylcarbonyl)methyl]-1H-tetrazole trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: PCl₅; quinoline / CHCl₃ / 2.5 h / 20 °C

2: 300 mg / hydrazoic acid / CHCl₃; benzene / 48 h / 20 °C

3: 76 percent / H₂ / 10 percent Pd/C / methanol / 5 h / 20 °C / 760 Torr

4: 75 percent / EDCI; HOBt; DIPEA / dimethylformamide / 24 h / 20 °C

5: 100 percent / H₂O / 0.5 h / 20 °C

With quinoline; hydrogen azide; phosphorus pentachloride; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; chloroform; water; N,N-dimethyl-formamide; benzene;