(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

Base Information

Chemical Name:(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole
CAS No.:417704-44-0
Molecular Formula:C₂₇H₂₇N₅O₄
Molecular Weight:485.542
Hs Code.:

Synonyms:(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

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Chemical Property of (2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

Chemical Property:

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Technology Process of (2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

There total 4 articles about (2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [(S)-3-Benzyloxycarbonylamino-1-chloro-4-phenyl-but-(Z)-ylideneamino]-acetic acid benzyl ester

: 417704-44-0
(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

Guidance literature:: With hydrogen azide; In chloroform; benzene; at 20 ℃; for 48h;

Reference yield:

: 15196-02-8
(S)-3-[(benzyloxycarbonyl)amino]-1-diazo-4-phenyl-2-butanone

: 417704-44-0
(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / acetonitrile / 24 h / Irradiation

2: PCl₅; quinoline / CHCl₃ / 2.5 h / 20 °C

3: 300 mg / hydrazoic acid / CHCl₃; benzene / 48 h / 20 °C

With quinoline; hydrogen azide; phosphorus pentachloride; triethylamine; In chloroform; acetonitrile; benzene; 1: Wolff rearrangement;

Reference yield:

: 2462-31-9
benzyl 2-aminoacetate hydrochloride

: 417704-44-0
(2S)-5-[2-(benzyloxycarbonylamino)-3-phenylpropyl]-1-(benzyloxycarbonylmethyl)-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / acetonitrile / 24 h / Irradiation

2: PCl₅; quinoline / CHCl₃ / 2.5 h / 20 °C

3: 300 mg / hydrazoic acid / CHCl₃; benzene / 48 h / 20 °C

With quinoline; hydrogen azide; phosphorus pentachloride; triethylamine; In chloroform; acetonitrile; benzene; 1: Wolff rearrangement;