2-(p-Anisidino)nicotinic acid hydrazide

Base Information

Chemical Name:2-(p-Anisidino)nicotinic acid hydrazide
CAS No.:77692-20-7
Molecular Formula:C13H14N4O2
Molecular Weight:258.2759
Hs Code.:
DSSTox Substance ID:DTXSID70228315
Nikkaji Number:J68.287J
Wikidata:Q83108281

Synonyms:2-(p-Anisidino)nicotinic acid hydrazide;BRN 5072624;Nicotinic acid, 2-(p-anisidino)-, hydrazide;77692-20-7;DTXSID70228315;2-(p-Anisidino)nicotinic hydrazide;2-(p-anisidino)-nicotinic acid hydrazide;LS-96525

Suppliers and Price of 2-(p-Anisidino)nicotinic acid hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(p-Anisidino)nicotinic acid hydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.289g/cm³
XLogP3:1.8
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:258.11167570
Heavy Atom Count:19
Complexity:292

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)NC2=C(C=CC=N2)C(=O)NN

Technology Process of 2-(p-Anisidino)nicotinic acid hydrazide

There total 4 articles about 2-(p-Anisidino)nicotinic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 51947-86-5
Methyl 2-(p-anisidino)-nicotinic acid

: 77692-20-7
2-(4-methoxyanilino)-3-pyridinecarbohydrazide

Guidance literature:: With hydrazine hydrate; for 5h; Heating;
DOI:10.1007/BF00765715

Reference yield: 78.0%

: 95774-49-5
ethyl 2-((4-methoxyphenyl)amino)nicotinate

: 77692-20-7
2-(4-methoxyanilino)-3-pyridinecarbohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1016/j.bmc.2006.10.027

Reference yield:

: 2942-59-8
2-chloronicotinic acid

: 77692-20-7
2-(4-methoxyanilino)-3-pyridinecarbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / 3 h / Heating

2: 80 percent / ethane-1,2-diol / 6 h / 160 °C

3: 78 percent / hydrazine hydrate / ethanol / 2 h / Heating

With sulfuric acid; hydrazine hydrate; In ethanol; ethylene glycol;
DOI:10.1016/j.bmc.2006.10.027