ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

Base Information

Chemical Name:ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate
CAS No.:1312479-36-9
Molecular Formula:C₂₀H₂₅NO₅S
Molecular Weight:391.488
Hs Code.:

Synonyms:ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

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Chemical Property of ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

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Technology Process of ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

There total 6 articles about ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312479-35-8
ethyl 4-(4-iodo-3-methyl-2-oxopyridin-1(2H)-yl)-2-methyl-2-(methylsulfonyl)butanoate

: 98-80-6
phenylboronic acid

: 1312479-36-9
ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

Guidance literature:: With potassium carbonate; PD EnCat; In 1,4-dioxane; water; at 20 - 80 ℃;

Reference yield:

: 153034-80-1
2-Fluoro-4-iodo-3-methylpyridine

: 1312479-36-9
ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; water / 1,4-dioxane / 1 h / 100 °C

2: caesium carbonate / tetrahydrofuran / 20 - 50 °C

3: potassium carbonate / PD EnCat_.(TM). / 1,4-dioxane; water / 20 - 80 °C

With hydrogenchloride; water; potassium carbonate; caesium carbonate; PD EnCat; In tetrahydrofuran; 1,4-dioxane; water;

Reference yield:

: 535-13-7
2-chloro-propanoic acid, ethyl ester

: 1312479-36-9
ethyl 2-methyl-4-(3-methyl-2-oxo-4-phenylpyridin-1(2H)-yl)-2-(methylsulfonyl)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 20 h / 77 °C

2.1: sodium hydride / N,N-dimethyl-formamide; hexane; mineral oil / 0.5 h / 20 °C / Inert atmosphere

2.2: 0 - 25 °C

3.1: caesium carbonate / tetrahydrofuran / 20 - 50 °C

4.1: potassium carbonate / PD EnCat_.(TM). / 1,4-dioxane; water / 20 - 80 °C

With sodium hydride; potassium carbonate; caesium carbonate; PD EnCat; In tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; N,N-dimethyl-formamide; mineral oil;