(η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Base Information

Chemical Name:(η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron
CAS No.:112295-32-6
Molecular Formula:C₂₁H₁₈FeO₄Si
Molecular Weight:418.304
Hs Code.:

Synonyms:(η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Suppliers and Price of (η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

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Chemical Property of (η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

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Technology Process of (η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

There total 2 articles about (η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 112218-89-0
(η4-exo-1-methyl-endo-1-chloro-2,5-diphenylsilacyclopentadiene)tricarbonyliron

: 112295-32-6
(η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Guidance literature:: With methanol; In methanol; MeOH, room temp., 3 h;
DOI:10.1016/0022-328X(87)85087-8

Reference yield: 71.0%

: 67-56-1
methanol

: 112218-89-0
(η4-exo-1-methyl-endo-1-chloro-2,5-diphenylsilacyclopentadiene)tricarbonyliron

: 112295-32-6
(η4-exo-1-methyl-endo-1-methoxy-2,5-diphenylsilacyclopentadiene)tricarbonyliron

Guidance literature:: In tetrachloromethane; addn. of MeOH to soln. of complex (cooled to 0°C), mixt. allowed to warm to room temp., reaction time 3h, exclusion of air and moisture, kinetics at -20.degee.C; solvent removed, recrystn. (hexane, -20°C); Kinetics;