N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline

Base Information

Chemical Name:N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline
CAS No.:38766-64-2
Molecular Formula:C₁₆H₁₆Cl₃NO₂
Molecular Weight:360.668
Hs Code.:
DSSTox Substance ID:DTXSID10959570
Nikkaji Number:J1.619.296A

Synonyms:N-(alpha-trichloromethyl-4-methoxybenzyl)-4-methoxyaniline;N-(alpha-trichloromethyl-p-methoxybenzyl)-p-methoxyaniline

Suppliers and Price of N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline

Chemical Property:

Vapor Pressure:4.8E-09mmHg at 25°C
Boiling Point:471.1°Cat760mmHg
Flash Point:238.7°C
Density:1.34g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:359.024662
Heavy Atom Count:22
Complexity:322

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(C(Cl)(Cl)Cl)NC2=CC=C(C=C2)OC

Technology Process of N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline

There total 5 articles about N-(alpha-Trichloromethyl-p-methoxybenzyl)-p-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-94-9
4-methoxy-aniline

: 38766-64-2
N-(4-Methoxyphenyl)-N-<2,2,2-trichloro-1-(4-methoxyphenyl)>-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / TiCl₄ / benzene / 2 h / Heating

2: N-chlorosuccinimide / CCl₄

3: 1.) BH₃*Me₂S, CH₂Cl₂, reflux, 16 h, 2.) 2N aqueous sodium hydroxide, r.t., 30 min

With N-chloro-succinimide; titanium tetrachloride; In tetrachloromethane; benzene;
DOI:10.1016/S0040-4020(01)86404-8

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 38766-64-2
N-(4-Methoxyphenyl)-N-<2,2,2-trichloro-1-(4-methoxyphenyl)>-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / TiCl₄ / benzene / 2 h / Heating

2: N-chlorosuccinimide / CCl₄

3: 1.) BH₃*Me₂S, CH₂Cl₂, reflux, 16 h, 2.) 2N aqueous sodium hydroxide, r.t., 30 min

With N-chloro-succinimide; titanium tetrachloride; In tetrachloromethane; benzene;
DOI:10.1016/S0040-4020(01)86404-8

Reference yield:

: 6325-62-8
N,1-bis(4-methoxyphenyl)ethan-1-imine

: 38766-64-2
N-(4-Methoxyphenyl)-N-<2,2,2-trichloro-1-(4-methoxyphenyl)>-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-chlorosuccinimide / CCl₄

2: 1.) BH₃*Me₂S, CH₂Cl₂, reflux, 16 h, 2.) 2N aqueous sodium hydroxide, r.t., 30 min

With N-chloro-succinimide; In tetrachloromethane;
DOI:10.1016/S0040-4020(01)86404-8