4-methoxy-N-[(1E)-1-(4-methoxyphenyl)ethylidene]aniline

Base Information

• Chemical Name: 4-methoxy-N-[(1E)-1-(4-methoxyphenyl)ethylidene]aniline
• CAS No.: 6325-62-8
• Molecular Formula: C16H17 N O2
• Molecular Weight: 255.316

Synonyms:p-Anisidine,N-(p-methoxy-a-methylbenzylidene)-(8CI); (4-Methoxyphenyl)[1-(4-methoxyphenyl)ethylidene]amine;4-Methoxy-N-[1-(4-methoxyphenyl)ethylidene]aniline; NSC 30992

Chemical Property of 4-methoxy-N-[(1E)-1-(4-methoxyphenyl)ethylidene]aniline

Chemical Property:

• Vapor Pressure: 2.75E-05mmHg at 25°C
• Boiling Point: 368.2°Cat760mmHg
• Flash Point: 143.2°C
• Density: 1.02g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methoxy-N-[(1E)-1-(4-methoxyphenyl)ethylidene]aniline

There total 7 articles about 4-methoxy-N-[(1E)-1-(4-methoxyphenyl)ethylidene]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-methoxy-aniline (104-94-9) + 4-methoxyphenylacetylen (768-60-5) → N,1-bis(4-methoxyphenyl)ethan-1-imine (6325-62-8)

Guidance literature:

With C₄₆H₇₀Br₄Hg₂N₂; In tetrahydrofuran; at 67 ℃; for 10h; regioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1039/c7dt04589a

Reference yield: 90.0%

4-methoxy-aniline (104-94-9) + 1-(4-methoxyphenyl)ethanone (100-06-1) → N,1-bis(4-methoxyphenyl)ethan-1-imine (6325-62-8)

Guidance literature:

In toluene; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.orglett.6b01509

Reference yield:

(±)-4-methoxy-N-(1-(4-methoxyphenyl)ethyl)aniline (471254-25-8) → N,1-bis(4-methoxyphenyl)ethan-1-imine (6325-62-8)

Guidance literature:

With manganese(IV) oxide; 2,6-dimethoxy-p-quinone; ruthenium; In toluene; for 4h; Heating;

DOI:10.1039/b202117j

upstream raw materials:

4-methoxy-aniline

1-(4-methoxyphenyl)ethanone

(±)-4-methoxy-N-(1-(4-methoxyphenyl)ethyl)aniline

4-methoxyphenylacetylen

Downstream raw materials:

N-(4-Methoxyphenyl)-N-<2,2,2-trichloro-1-(4-methoxyphenyl)>-ethylamine

C₂₆H₃₂ClIrNO₂

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