6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:74653-32-0
Molecular Formula:C₃₁H₄₂N₂O₉
Molecular Weight:586.682
Hs Code.:

Synonyms:6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 6 articles about 6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 74653-31-9
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-3-O-benzyl-2-deoxy-β-D-glucopyranoside

: 75-36-5
acetyl chloride

: 74653-32-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In chloroform; at 80 ℃; for 24h;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

: 74653-32-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

2: 1.) BaO-Ba(OH)2*8H₂O; 2.) acetic acid / 1.) DMF, 0 deg C, 4 h; 2.) 10 h, 55 deg C

3: 61 percent / imidazole / CHCl₃ / 24 h / 80 °C

With 1H-imidazole; barium dihydroxide; toluene-4-sulfonic acid; acetic acid; barium(II) oxide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 62205-56-5,159173-77-0
6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside

: 74653-32-0
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-6-O-acetyl-3-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / sodium methoxide / methanol / 24 h

2: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

3: 1.) BaO-Ba(OH)2*8H₂O; 2.) acetic acid / 1.) DMF, 0 deg C, 4 h; 2.) 10 h, 55 deg C

4: 61 percent / imidazole / CHCl₃ / 24 h / 80 °C

With 1H-imidazole; barium dihydroxide; sodium methylate; toluene-4-sulfonic acid; acetic acid; barium(II) oxide; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85520-2