N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine

Base Information

• Chemical Name: N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine
• CAS No.: 1555819-53-8
• Molecular Formula: C₂₈H₃₄N₂O₄
• Molecular Weight: 462.589
• Mol file: 1555819-53-8.mol

Synonyms:N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine

Chemical Property of N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine

There total 3 articles about N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

5-allyl-2-hydroxy-3-methoxybenzaldehyde (22934-51-6) + rac-diaminocyclohexane (694-83-7) → N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine (1555819-53-8)

Guidance literature:

In ethanol; at 20 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c3tc31814a

Reference yield:

3-methoxy-2-hydroxybenzaldehyde (148-53-8) → N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine (1555819-53-8)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate

2: toluene; N,N-dimethyl-aniline / 5 h / 215 °C / Sealed tube

3: ethanol / 12 h / 20 °C / Inert atmosphere; Schlenk technique

With potassium carbonate; In ethanol; N,N-dimethyl-aniline; toluene;

DOI:10.1039/c3tc31814a

Reference yield:

2-allyloxy-3-methoxy-benzaldehyde (23343-06-8) → N,N'-bis(5-allyl-3-methoxysalicylidene)cyclohexane-1,2-diamine (1555819-53-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene; N,N-dimethyl-aniline / 5 h / 215 °C / Sealed tube

2: ethanol / 12 h / 20 °C / Inert atmosphere; Schlenk technique

In ethanol; N,N-dimethyl-aniline; toluene;

DOI:10.1039/c3tc31814a

upstream raw materials:

5-allyl-2-hydroxy-3-methoxybenzaldehyde

rac-diaminocyclohexane

2-allyloxy-3-methoxy-benzaldehyde

3-methoxy-2-hydroxybenzaldehyde