2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

Base Information

Chemical Name:2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate
CAS No.:1370007-67-2
Molecular Formula:C₂₈H₃₅NO₇SSi
Molecular Weight:557.74
Hs Code.:

Synonyms:2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

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Chemical Property of 2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

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Technology Process of 2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

There total 4 articles about 2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-hydroxyacrylonitrile

: 124-63-0
methanesulfonyl chloride

: 1370007-67-2
2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1.16667h;

Reference yield:

: 1370007-62-7
2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)acetonitrile

: 1370007-67-2
2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 20 °C

2: trifluoroacetic acid / chloroform; water / 20 °C

3: triethylamine / dichloromethane / 1.17 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 1370007-65-0
2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-(dimethylamino)acrylonitrile

: 1370007-67-2
2-((3aS,6R,6aR)-6-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-2-cyanovinyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / chloroform; water / 20 °C

2: triethylamine / dichloromethane / 1.17 h / 0 °C

With triethylamine; trifluoroacetic acid; In dichloromethane; chloroform; water;