C₁₄H₁₉BrN₂O₃

Base Information

Chemical Name:C₁₄H₁₉BrN₂O₃
CAS No.:1616606-35-9
Molecular Formula:C₁₄H₁₉BrN₂O₃
Molecular Weight:343.22
Hs Code.:

C<sub>14</sub>H<sub>19</sub>BrN<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₄H₁₉BrN₂O₃

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Chemical Property of C₁₄H₁₉BrN₂O₃

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Technology Process of C₁₄H₁₉BrN₂O₃

There total 5 articles about C₁₄H₁₉BrN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-75-1
pyrrolidine

: 1215858-80-2
2-bromo-1-(2-bromo-4,5-dimethoxyphenyl)ethanone oxime

: 1616606-35-9
C₁₄H₁₉BrN₂O₃

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 6286-46-0
2-bromo-4,5-dimethoxybenzoic acid

: 1616606-35-9
C₁₄H₁₉BrN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4.5 h / 20 °C / Inert atmosphere; Cooling with ice

2: tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

3: copper(I) bromide / ethyl acetate; chloroform / 2.5 h / Inert atmosphere; Reflux

4: hydroxylamine hydrochloride / water; methanol / 20 °C / Inert atmosphere

5: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; copper(I) bromide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; ethyl acetate;

Reference yield:

: 2-bromo-4,5-dimethoxy-N-methoxy-N-methyl-2-vinylbenzamide

: 1616606-35-9
C₁₄H₁₉BrN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

2: copper(I) bromide / ethyl acetate; chloroform / 2.5 h / Inert atmosphere; Reflux

3: hydroxylamine hydrochloride / water; methanol / 20 °C / Inert atmosphere

4: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; copper(I) bromide; In tetrahydrofuran; methanol; chloroform; water; ethyl acetate;