Technology Process of C20H13Cl2F3N2O3
There total 10 articles about C20H13Cl2F3N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-Bromosuccinimide / tetrachloromethane / 18 h / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 60 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
4: manganese(IV) oxide / chloroform / Reflux
With
manganese(IV) oxide; N-Bromosuccinimide; lithium aluminium tetrahydride; potassium carbonate;
In
tetrahydrofuran; tetrachloromethane; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C
2: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C
3: triethylamine / 20 °C
4: diisobutylaluminium hydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
5: thionyl chloride; 1,2,3-Benzotriazole / dichloromethane / 0 - 20 °C
6: potassium carbonate / N,N-dimethyl-formamide / 60 °C
7: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
8: manganese(IV) oxide / chloroform / Reflux
With
1,2,3-Benzotriazole; manganese(IV) oxide; N-chloro-succinimide; lithium aluminium tetrahydride; thionyl chloride; hydroxylamine hydrochloride; diisobutylaluminium hydride; potassium carbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
