di-β,β'-chloroethyl phenylphosphinate

Base Information

Chemical Name:di-β,β'-chloroethyl phenylphosphinate
CAS No.:35411-10-0
Molecular Formula:C₁₀H₁₃Cl₂O₂P
Molecular Weight:267.092
Hs Code.:

Synonyms:di-β,β'-chloroethyl phenylphosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-β,β'-chloroethyl phenylphosphinate

Chemical Property:

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Technology Process of di-β,β'-chloroethyl phenylphosphinate

There total 6 articles about di-β,β'-chloroethyl phenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 75-21-8,99932-75-9
oxirane

: 644-97-3
Dichlorophenylphosphine

: 35411-10-0
di-β,β'-chloroethyl phenylphosphinate

: 3450-36-0
β-chloroethyl β-chloroethylphenylphosphinate

Guidance literature:: In benzene; for 1h; Ambient temperature;

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 107-07-3
2-chloro-ethanol

: 35411-10-0
di-β,β'-chloroethyl phenylphosphinate

: 17986-57-1
β-chloroethyl phenylphosphinate

: 13547-39-2
di(β-chloroethyl) phenylphosphonate

Guidance literature:: With triethylamine; In benzene; at -5 - 40 ℃; for 1h; Inert atmosphere;
DOI:10.1134/S1070428016030052

Reference yield:

: 18157-17-0
(2-chloroethoxy)trimethylsilane

: 105-39-5
chloroacetic acid ethyl ester

: 644-97-3
Dichlorophenylphosphine

: 35411-10-0
di-β,β'-chloroethyl phenylphosphinate

: C₁₂H₁₆ClO₄P

Guidance literature:: (2-chloroethoxy)trimethylsilane; chloroacetic acid ethyl ester; Dichlorophenylphosphine; In dichloromethane; at -5 - 0 ℃; for 0.5h; Inert atmosphere;

In dichloromethane; at 80 - 100 ℃; for 3h; Inert atmosphere;
DOI:10.1134/S1070428016030052