(3-methylcyclohexyl)zinc iodide

Base Information

Chemical Name:(3-methylcyclohexyl)zinc iodide
CAS No.:1285537-31-6
Molecular Formula:C₇H₁₃IZn
Molecular Weight:289.475
Hs Code.:

Synonyms:(3-methylcyclohexyl)zinc iodide

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Chemical Property of (3-methylcyclohexyl)zinc iodide

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Technology Process of (3-methylcyclohexyl)zinc iodide

There total 2 articles about (3-methylcyclohexyl)zinc iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66922-06-3,66922-07-4,89894-77-9
1-iodo-3-methylcyclohexane

: 7440-66-6
zinc

: 1285537-31-6
(3-methylcyclohexyl)zinc iodide

Guidance literature:: With chloro-trimethyl-silane; lithium chloride; In tetrahydrofuran; ethylene dibromide; at 25 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201914490

Reference yield:

: 591-23-1
m-methylcyclohexanol

: 1285537-31-6
(3-methylcyclohexyl)zinc iodide

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; triphenylphosphine; 1-methyl-1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

2: lithium chloride; chloro-trimethyl-silane / tetrahydrofuran; ethylene dibromide / 25 °C / Inert atmosphere; Schlenk technique

With 1-methyl-1H-imidazole; chloro-trimethyl-silane; iodine; triphenylphosphine; lithium chloride; In tetrahydrofuran; dichloromethane; ethylene dibromide;
DOI:10.1002/anie.201914490

Reference yield: 85.0%

: 1285537-31-6
(3-methylcyclohexyl)zinc iodide

: 100366-75-4
2‐iodo‐5‐(trifluoromethyl)pyridine

: C₁₃H₁₆F₃N

Guidance literature:: 2‐iodo‐5‐(trifluoromethyl)pyridine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 25 ℃; for 0.166667h; Inert atmosphere;

(3-methylcyclohexyl)zinc iodide; In tetrahydrofuran; 1-ethyl-2-pyrrolidinone; at 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1038/nchem.505