1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

Base Information

Chemical Name:1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione
CAS No.:1347750-39-3
Molecular Formula:C₂₃H₂₂O₈
Molecular Weight:426.423
Hs Code.:

Synonyms:1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

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Chemical Property of 1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

Chemical Property:

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Technology Process of 1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

There total 4 articles about 1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 2-(4-((1E,6E)-7-(4-hydroxy-3-methoxyphenyl)-3,5-dioxohepta-1,6-dien-1-yl)-2-methoxyphenoxy)acetate

: 1347750-39-3
1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

Guidance literature:: With sodium hydroxide; In acetone; Inert atmosphere;
DOI:10.1016/j.bmcl.2016.06.079

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1347750-39-3
1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trioxide / ethyl acetate / 1 h / 70 °C / Inert atmosphere

1.2: 0.5 h / 70 °C / Inert atmosphere

2.1: boron trioxide / ethyl acetate / 1 h / 70 °C / Inert atmosphere

2.2: 0.5 h / 70 °C / Inert atmosphere

3.1: sodium hydroxide / acetone / Inert atmosphere

With boron trioxide; sodium hydroxide; In ethyl acetate; acetone;
DOI:10.1016/j.bmcl.2016.06.079

Reference yield:

: 51264-70-1
ethyl 2-(4-formyl-2-methoxyphenoxy)acetate

: 1347750-39-3
1-(3-methoxy-4-hydroxyphenyl)-7-(4-oxoacetoxy-3-methoxyphenyl)-1,6-heptadiene-3,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trioxide / ethyl acetate / 1 h / 70 °C / Inert atmosphere

1.2: 0.5 h / 70 °C / Inert atmosphere

2.1: sodium hydroxide / acetone / Inert atmosphere

With boron trioxide; sodium hydroxide; In ethyl acetate; acetone;
DOI:10.1016/j.bmcl.2016.06.079