(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄

Base Information

• Chemical Name: (CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄
• CAS No.: 180320-94-9
• Molecular Formula: BF₄*C₄₈H₄₅O₄P₃Re
• Molecular Weight: 1051.82

Synonyms:(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄

Chemical Property of (CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄

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Technology Process of (CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄

There total 1 articles about (CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)⁽¹⁺⁾*BF₄^(1-)=[(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(CC(H)COOC₂H₅)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(CH3C(CH2P(C6H5)2)3)Re(CO)2(H) (166989-33-9) + tetrafluoroboric acid dimethyl ether complex (67969-83-9) + propynoic acid ethyl ester (623-47-2) → (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*BF4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)]BF4 (180320-94-9)

Guidance literature:

With HBF₄ * OMe₂; In dichloromethane; N2-atmosphere; stirring (-10°C to room temp.); evapn. (vac.), extg. (THF), EtOH addn., concg. (N2-stream); elem. anal.;

DOI:10.1021/om9602264

Reference yield: 72.0%

ethanol (64-17-5) + (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)(1+)*BF4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(H)COOC2H5)]BF4 (180320-94-9) → (CH3C(CH2P(C6H5)2)3)Re(CO)2(CC(CH2COOC2H5)OC2H5)(1+)*B(C6H5)4(1-)=[(CH3C(CH2P(C6H5)2)3)Re(CO)2(C8H12O3)][B(C6H5)4]

Guidance literature:

In dichloromethane; N2-atmosphere; stirring (room temp., overnight); crystn. on EtOH / Et2O (1 : 2) addn.; elem. anal.;

DOI:10.1021/om9602264

upstream raw materials:

(CH₃C(CH₂P(C₆H₅)2)3)Re(CO)2(H)

tetrafluoroboric acid dimethyl ether complex

propynoic acid ethyl ester

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