ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Base Information

Chemical Name:ethyl bis[m-(phenylazo)benzyl]isocyanoacetate
CAS No.:1361123-00-3
Molecular Formula:C₃₁H₂₇N₅O₂
Molecular Weight:501.588
Hs Code.:

Synonyms:ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Suppliers and Price of ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

There total 5 articles about ethyl bis[m-(phenylazo)benzyl]isocyanoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2999-46-4
Ethyl isocyanoacetate

: 1361122-99-7
1-(3-(bromomethyl)phenyl)-2-phenyldiazene

: 1361123-00-3
ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile; at 50 ℃; for 48h;
DOI:10.1002/chem.201102609

Reference yield:

: 65926-75-2
(3-(phenyldiazenyl)phenyl)methanol

: 1361123-00-3
ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 0 - 45 °C

2: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / acetonitrile / 48 h / 50 °C

With N-Bromosuccinimide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201102609

Reference yield:

: 586-96-9
Nitrosobenzene

: 1361123-00-3
ethyl bis[m-(phenylazo)benzyl]isocyanoacetate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 48 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / 0 - 40 °C / Inert atmosphere

3: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 0 - 45 °C

4: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / acetonitrile / 48 h / 50 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; acetic acid; triphenylphosphine; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.201102609