1-(4-methoxyphenyl)-4-phenylnaphthalene

Base Information

Chemical Name:1-(4-methoxyphenyl)-4-phenylnaphthalene
CAS No.:1170321-07-9
Molecular Formula:C₂₃H₁₈O
Molecular Weight:310.395
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-4-phenylnaphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxyphenyl)-4-phenylnaphthalene

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Technology Process of 1-(4-methoxyphenyl)-4-phenylnaphthalene

There total 6 articles about 1-(4-methoxyphenyl)-4-phenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 4-phenylnaphthalen-1-yl 4-nitrobenzenesulfonate

: 5720-07-0
4-methoxyphenylboronic acid

: 1170321-07-9
1-(4-methoxyphenyl)-4-phenylnaphthalene

Guidance literature:: With potassium phosphate; palladium diacetate; XPhos; In tetrahydrofuran; at 80 ℃; for 18h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tet.2016.02.061

Reference yield:

: 2996-92-1,46143-12-8
phenyl trimethylsiloxane

: C₁₇H₁₃FO

: 1170321-07-9
1-(4-methoxyphenyl)-4-phenylnaphthalene

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; tricyclohexylphosphine; In 2-methyltetrahydrofuran; at 80 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1002/cctc.202001462

Reference yield:

: 604-44-4
4-chloronaphthalen-1-ol

: 1170321-07-9
1-(4-methoxyphenyl)-4-phenylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: potassium phosphate; palladium diacetate; XPhos / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Sealed tube

3: potassium phosphate; palladium diacetate; XPhos / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Sealed tube

With potassium phosphate; palladium diacetate; N-ethyl-N,N-diisopropylamine; XPhos; In tetrahydrofuran; dichloromethane; 2: |Suzuki-Miyaura Coupling / 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2016.02.061